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Beilstein J. Org. Chem. 2018, 14, 583–592, doi:10.3762/bjoc.14.45
Graphical Abstract
Figure 1: Commercially available antimalarial drugs.
Scheme 1: Current batch syntheses of the key intermediate 5-(ethyl(2-hydroxyethyl)amino)pentan-2-one (6).
Scheme 2: Retrosynthetic strategy to hydroxychloroquine (1).
Scheme 3: Schematic representation for continuous in-line extraction of 10.
Scheme 4: Optimization of the flow process for the synthesis of 12.